Programmable microwave chemical reactor

The X O series programmable computer microwave catalytic synthesis and extraction system is a new type of chemical reaction device that uses microwave technology as a physical catalytic means. It mainly consists of a microwave catalytic analyzer host, a microcomputer touch screen intelligent control system, a high-precision infrared temperature sensor, a refrigeration cycle machine (optional), and a system integrating sample addition and reflux condensation devices. The organic synthesis reactions that have been studied and achieved results include: substitution, addition, elimination, esterification, hydrolysis, addition polymerization, condensation polymerization, oxidation, reduction and other polymer reactions. For the convenience of storing and comparing different reaction environments, the program can be programmed into 5 sets of reaction programs to set reaction parameters. During the reaction process, the changes in reaction parameters can be observed, and the temperature of the reactants can be displayed in real time. The entire reaction process can be observed in real time through a color LCD display. An optional computer connection software is also available, which can display and record various reaction parameters in real time on the computer, and store unlimited reaction program solutions. Xianou Company has also added an optional large memory camera for full dynamic recording function, making it easy to record and capture various colorful reaction states.
The instrument adopts a large capacity stainless steel chamber to prevent magnetic materials from entering the chamber and is corrosion-resistant. Infrared temperature sensor for real-time and accurate monitoring of reaction temperature; Adopting innovative computer self-learning technology, also known as temperature automatic frequency conversion control technology, the temperature control accuracy reaches ± 1 ℃, realizing non pulse microwave continuous emission and automatic adjustment of microwave power. By inducing or accelerating chemical reactions and physical processes through enthalpy and entropy effects, reaction rates have been increased by hundreds to thousands of times, while reaction yields have been increased, making many previously difficult to generate or slow chemical reaction substances or physical processes easier to achieve and complete at high speeds. Suitable for fields such as organic synthesis chemistry, inorganic synthesis chemistry, pharmaceutical chemistry, food science, quarantine and epidemic prevention, military chemistry, molecular biology, analytical chemistry, petrochemicals, materials science, biomedicine, metallurgy, environmental pollution control, etc.
Programmable computer microwave catalysis/synthesis/extraction system (large and highly sensitive touch screen operation)

System features:

Adopting Panasonic microwave generation system, with stable performance; Microwave power can be fine tuned; Microwave frequency: 2450MHz;
The reaction vessel can be optionally equipped with a uniquely designed cooling water device function, which can effectively control the high temperature produced by microwave emission, achieve a 100% utilization rate of microwaves, and enable the reactants to obtain the maximum microwave effect under the set reaction conditions, ensuring the uniformity and high yield of reaction products;
The parameter control part adopts a large and high-sensitivity touch screen operation, with programmable control of all parameters and storage of five sets of experimental data;
Equipped with a 10 inch ultra-thin, ultra high definition, multifunctional LCD large screen display, real-time display of sample working status, optional connection with a large memory camera for full dynamic recording function, easy recording and capturing of various exciting reaction states of various images;
Adopting high-precision non-contact infrared temperature measurement, real-time detection of reaction temperature, accurate control of reaction process temperature, control range: room temperature~500 ℃;
Adopting innovative computer self-learning technology, also known as temperature automatic frequency conversion control technology, the temperature control accuracy reaches ± 1 ℃, realizing non pulse microwave continuous emission and automatically adjusting microwave power;
Adopting a unique variable frequency blower cooling function to maintain uniform temperature inside the chamber;
● Reaction vessels such as glass and polytetrafluoroethylene can be selected;
● Optional magnetic and mechanical stirring devices;
Optional computer connection software can be used to display and record various reaction parameters in real-time on the computer, and store unlimited reaction program solutions;
Users can install standard interface reaction containers and injection, ventilation, separation and other devices according to the reaction conditions;
● Equipped with super temperature and sensor abnormality protection, high reliability and safety;
Adopting a stainless steel inner shell with anti magnetism to prevent magnetic materials from entering the cavity and breaking the internal structure, it is durable and long-lasting;
The microwave leakage of the whole machine meets national standards and has passed the electromagnetic radiation safety certification of the Provincial Institute of Metrology and the CE certification of the European Union;
Shanghai Institute of Ceramics, Chinese Academy of Sciences, School of Environmental Science and Engineering, Tongji University, Department of Materials Science and Engineering, School of Chemical Engineering, Nanjing University of Science and Technology, School of Materials Science and Engineering, Nanjing University of Technology, Kunming Institute of Entomology and Botany, Chinese Academy of Forestry, School of Chemical Engineering, Nanjing University of Science and Technology, Jiangsu Academy of Building Sciences, Subot New Materials Research Center, School of Chemical and Bioengineering, Yancheng University of Technology, School of Pharmaceutical and Chemical Engineering, Taizhou University, Nanomaterials Research Center, Nanjing University of Aeronautics and Astronautics, and other relevant units have adopted the modified equipment and published articles, such as: Guoan Tai andWanlin Guo, Sonochemistry-Assisted Microwave Synthesis and Optical Study ofSingle-Crystalline CdS Nanoflowers, Ultrasonic Sonochemistry, 2008, 15:350~356. (SCI, IF=2.434) （ Research on Nanomaterial Preparation) Nanjing University of Aeronautics and Astronautics Nanomaterial Research Center.