Ultrasonic ultra-high pressure polymerization reaction system

Product Description

The ATPIO series ultrasonic ultra-high pressure polymerization reaction system is developed by our company after many years of experience. In the field of chemical preparation and testing, it is the first to combine ultrasonic and high-pressure technology without interference, realizing the synergistic treatment of ultrasonic and high-pressure reactions. Based on this technology, the excellent characteristics of ultrasound, including mechanical effects, thermal effects, physicochemical effects (including dispersion, thixotropy, cavitation), good directionality, and strong penetration ability, can not only improve the diffusion rate of fluids in reactants, but also play a role in heterogeneous nucleation. The product has functions such as ultrasonic and pressure regulation, timing, quantitative and temperature control. Suitable for rapid, efficient, and targeted synthesis of specified chemical monomers and target mixtures, applicable in fields involving the extraction of active ingredients in traditional Chinese medicine, synthesis of organic-inorganic compounds, drug intermediates, and nanomaterials, development of energy fuels and their new energy products. The processing has the characteristics of high chemical selectivity, high extraction efficiency, low loss rate of active ingredients, and high product crystallinity. In the preparation process of organic compounds, inorganic compounds, polymer polymerization, and metal nanomaterials, uniform sizing synthesis has been achieved, and non target reactions such as side reactions and chain reactions involving organic compounds can be effectively overcome.
Characteristics of ultrasonic ultra-high pressure polymerization reaction system:
The device has optional ultrasonic frequency and quantity, adjustable internal volume and gas release rate of the reaction kettle, and is equipped with mechanical stirring, rapid heating functions, etc. Based on the basic principles of fluid mechanics and mechanical science, the device adopts variable frequency stirring technology, combined with the cavitation effect of the ultrasonic system, to achieve turbulent and highly uniform flow and temperature fields in the kettle.
Selection table for ultrasonic ultra-high pressure polymerization reaction system:

Features

Product features:
The Nanjing Xianou XO-GY series ultrasonic ultra-high pressure polymerization reaction system has separate control and collaborative functions of ultrasonic and reactor pressure.
Adopting a foreign focused ultrasonic generation system with stable performance; Ultrasonic power can be fine tuned; Ultrasonic frequency: 25KHz, the ultrasonic frequency range can be selected from 15-40KHz, and the ultrasonic probe can be selected to intervene or not in the sample, acting on the sample function through cavitation effect or air transmission.
The high-pressure reactor can be optionally equipped with SUS304 stainless steel with PTFE coating corrosion-resistant material, which can be used for ultra-low temperature vacuum drying or other anhydrous reactions, low-temperature reactions, polymerization reactions, etc. through a low-temperature cooling vacuum pump system;
Polytetrafluoroethylene digestion function with temperature (or pressure) control and magnetic stirring (hydrothermal synthesis reactor);
The reaction vessel can be optionally equipped with a uniquely designed cooling water device, which can control the temperature from -70 to 500 ℃, the world's first;
Equipped with a high-precision platinum sensing temperature measurement system, it can accurately detect the reaction temperature in real time and control the reaction process temperature accurately; Control range: room temperature -400 ℃, temperature control accuracy: ≤ ±1℃；
Ultrasonic working time: can work continuously, adjustable from 0-9999S;
The reaction kettle can be optionally equipped with programmable temperature control function;
Various ultrasound probe diameters: Φ 12, Φ 15, Φ 18, Φ 25, Φ 30, Φ 35 suitable for reaction vessels of different capacities;
Equipped with mechanical stirring functions at different speeds, the speed can be adjusted;
The instrument adopts a closed reaction system and can be equipped with drip funnels and condenser tubes (optional) for reflux reactions. It can also achieve online analysis of environmental, biological, pharmaceutical and other samples;
● Equipped with super temperature and sensor abnormality protection, high reliability and safety;
Can be applied to laboratory research and enterprise production in biology, medicine, chemistry, pharmaceuticals, food, cosmetics, environmental protection, etc;
The entire instrument is made of domestic and foreign technology and materials, and has passed the EU Electrical Safety CE certification, with certificates.

Detailed configuration list

Department of Chemical Engineering of Tsinghua University, School of Aerospace and Materials Engineering of National University of Defense Technology, Shanghai Silicate Institute of Chinese Academy of Sciences, School of Materials Science and Engineering of Huazhong University of Science and Technology, State Key Laboratory of Natural Active Substances and Functions of China Pharmaceutical University, School of Food of Jiangnan University, School of Food of Henan University of Technology, School of Materials Science and Engineering of Henan Institute of Light Industry, Shandong Academy of Agricultural Sciences, Key Laboratory of Natural Medicine Chemistry of the Ministry of Education of Shaanxi Normal University, School of Environmental Science and Engineering of Tongji University, School of Materials Science and Engineering of East China University of Science and Technology, Department of Materials Science and Engineering of Nanjing University, School of Chemical Engineering of Nanjing University of Science and Technology, School of Materials Science and Engineering of Nanjing University of Technology, Kunming Institute of Insect Plants of Chinese Academy of Forestry Sciences, and School of Chemical Engineering of Nanjing University Relevant units such as Jiangsu Academy of Building Sciences and Nanjing University of Aeronautics and Astronautics Nanomaterials Research Center have adopted modified equipment and published articles, such as:

1、Guoan Tai and Wanlin Guo, Sonochemistry-Assisted Microwave Synthesisand Optical Study of Single-Crystalline CdS Nanoflowers, UltrasonicSonochemistry, 2008, 15: 350~356. (SCI, IF=2.434) (Research on Nanomaterial Preparation) Nanomaterial Research Center, Nanjing University of Aeronautics and Astronautics

2、Xiaoguo Liu, Kaili Lin, Chengtie Wu, Yueyue Wang, Zhaoyong Zou andJiang Chang, Multilevel Hierarchically Ordered Artificial Biomineral, Small,DOI: 10.1002/smll.201301633. SCI  Influencing factors=7.823