Ultrasonic microwave synergistic reaction workstation

Product Description

The XO-SM series ultrasonic microwave synergistic reaction system is a new product developed through years of cooperation between our company and Nanjing University of Aeronautics and Astronautics. In the field of chemical preparation and detection, it combines ultrasound and microwave technology without interference, achieving synergistic processing of ultrasound and microwave. Based on this technology, the XO-SM series products have functions such as independent adjustable ultrasonic and microwave power, timed and temperature controlled full window control, etc. Suitable for rapid, efficient, and targeted synthesis of specified chemical monomers and target mixtures, applicable in fields involving the extraction of active ingredients in traditional Chinese medicine, synthesis of organic-inorganic compounds, drug intermediates, and nanomaterials, development of energy fuels and their new energy products. The processing has the characteristics of high chemical selectivity, high extraction efficiency, low loss rate of active ingredients, and high product crystallinity. In addition, it achieves uniform size synthesis in inorganic polymer polymerization and preparation of metal nanomaterials, and can effectively overcome non target reactions such as side reactions and chain reactions involving organic compounds.

Nanjing Xianou Instrument Manufacturing Co., Ltd. [XO Series New Ultrasonic Microwave Synergistic Reaction System]

The ultrasonic microwave combined reaction system includes ultrasonic device, microwave device, circulating chiller (optional), lifting device, condensation reflux device, visual operation interface, fiber optic temperature measurement accessories, program controlled refrigeration or superconducting cooling device, etc. The ultrasonic device includes an ultrasonic probe, ultrasonic transducer, ultrasonic power supply, ultrasonic temperature control display, ultrasonic time control display, and ultrasonic power control display; Microwave devices include magnetrons, waveguides, microwave temperature control displays, microwave time control displays, and microwave power control displays; The circulating chiller device includes a temperature control display (maximum low operating temperature (-80 ℃), a time display controller, and a circulating pump; The condensing device includes a reflux condenser, a triangular bottle, a glass conduit, a sealing plug, and a circulating insulation material; The visual operation interface includes a visual control system and a real-time reaction monitoring system; Fiber optic temperature measurement accessories include foreign fiber optic temperature measurement equipment and platinum resistance sensor components; The refrigeration and superconducting cooling device includes a program-controlled refrigeration and superconducting rapid cooling system.

Features

System features:
The Nanjing Xianou XO-SM series ultrasonic microwave collaborative reaction system has separate control and collaborative functions for microwave, ultrasonic, and microwave ultrasonic. The system simultaneously implements functions such as visual interface control, high-precision program temperature control, multi-channel data storage, and directional transmission.
Adopting a foreign pulse microwave generation system with stable performance; Microwave power can be fine tuned; Microwave frequency: 2450MHz;
The ultrasound power can be fine tuned; Ultrasonic frequency: 25KHz, the ultrasonic frequency range can be selected from 15-40KHz, and the ultrasonic probe can be selected to intervene or not in the sample, acting on the sample function through cavitation effect or air transmission.
The ultrasonic transducer has an automatic lifting function, which can accurately control the immersion level according to experimental requirements. The vertical lifting immersion level accuracy is ± 0.1mm
Equipped with a UV catalytic device, wavelength: 253.7nm, power: 200W.
The reaction kettle can be equipped with polytetrafluoroethylene or high-temperature and corrosion-resistant glass materials, and can be used for ultra-low temperature microwave vacuum drying or other anhydrous reactions, low-temperature reactions, polymerization reactions, etc. through a low-temperature cooling vacuum pump system;
● Optional PTFE digestion tank (hydrothermal synthesis reactor) with temperature (or pressure) control and magnetic stirring or oscillation device;
The reaction vessel can be optionally equipped with a uniquely designed cooling water device, which can control the temperature from -40 to 500 ℃, the world's first; It can effectively control the high temperature generated by microwave emission, achieve a 100% utilization rate of microwaves, and maximize the microwave effect on the reactants under the set reaction conditions, ensuring the uniformity and high yield of reaction products;
The parameter control part adopts a high-sensitivity touch screen operating system, with programmable control of all parameters and storage of five sets of experimental data;
The instrument is equipped with a 10 inch ultra-thin, ultra high definition, multifunctional LCD large screen display, which displays the real-time working status of the sample;
Optional high-precision non-contact infrared temperature measurement or contact fiber optic, platinum sensing temperature measurement system, real-time and accurate detection of reaction temperature, accurate control of reaction process temperature; Control range: 0-500 ℃, temperature control accuracy: ≤ ±1℃；
Adopting a unique variable frequency blower cooling and program-controlled refrigeration device to maintain a constant temperature inside the chamber;
● Working hours: Can work continuously, adjustable between 0-9999s;
Microwave and ultrasound can be programmed for temperature control, timing, and power adjustment simultaneously;
Various ultrasound probe diameters: Φ 2, Φ 3, Φ 10, Φ 15, Φ 18, Φ 25, Φ 30, Φ 35, suitable for reaction vessels of different diameters;
Equipped with magnetic stirring, oscillation, and sample lifting devices of different speeds for use in conjunction with microwaves;
The instrument comes with a glass tube and a fluorine gel tube, and adopts an open reaction system. It can be equipped with a drip funnel and a condenser tube for reflux reaction, and can also achieve online analysis of environmental, biological, pharmaceutical and other samples;
● Equipped with super temperature and sensor abnormality protection, high reliability and safety;
Adopting a stainless steel inner shell with anti magnetism to prevent magnetic materials from entering the cavity and breaking the internal structure, it is durable and long-lasting;
Can be applied to laboratory research and enterprise production in biology, medicine, chemistry, pharmaceuticals, food, cosmetics, environmental protection, etc;
The entire instrument is made of domestic and foreign technologies and materials. The microwave reactor leakage of the whole machine meets international standards and has passed the electromagnetic radiation safety certification of the Provincial Institute of Metrology. And it has passed the EU Electrical Safety CE certification, equipped with certificates.

Selection table：

Department of Chemical Engineering of Tsinghua University, School of Aerospace and Materials Engineering of National University of Defense Technology, Shanghai Silicate Institute of Chinese Academy of Sciences, School of Materials Science and Engineering of Huazhong University of Science and Technology, State Key Laboratory of Natural Active Substances and Functions of China Pharmaceutical University, School of Food of Jiangnan University, School of Food of Henan University of Technology, School of Materials Science and Engineering of Henan Institute of Light Industry, Shandong Academy of Agricultural Sciences, Key Laboratory of Natural Medicine Chemistry of the Ministry of Education of Shaanxi Normal University, School of Environmental Science and Engineering of Tongji University, School of Materials Science and Engineering of East China University of Science and Technology, Department of Materials Science and Engineering of Nanjing University, School of Chemical Engineering of Nanjing University of Science and Technology, School of Materials Science and Engineering of Nanjing University of Technology, Kunming Institute of Insect Plants of Chinese Academy of Forestry Sciences, and School of Chemical Engineering of Nanjing University Relevant units such as Jiangsu Academy of Building Sciences and Nanjing University of Aeronautics and Astronautics Nanomaterials Research Center have adopted modified equipment and published articles, such as:

1、Xiaoguo Liu, Kaili Lin, Chengtie Wu, Yueyue Wang, Zhaoyong Zou and Jiang Chang, Multilevel Hierarchically Ordered Artificial Biomineral,Small, DOI: 10.1002/smll.201301633. SCIInfluencing factors=7.823(Shanghai Institute of Silicate, Chinese Academy of Sciences）

2、Daming Fan, Wenrui Ma, Liyun Wang, Jianlian Huang, Jianxin Zhao ,Hao Zhang, Wei Chen*. Determination of structural changes in microwavedrice starch using Fourier transform infrared and Raman spectroscopy. STARCH-STARKE, 2012, 64(8): 598-606，SCI,IF=1.243Gangnam University Food Academy

3、Xiao-Lan Cheng, Jin-Yi Wan, Ping Li，Lian-Wen Qi. Ultrasonic/microwave assisted  extraction and diagnostic ion filtering strategy by liquid chromatography–quadrupole time-of-flight mass spectrometry for rapid characterization of flavonoids in Spatholobus  suberectus. Journal of Chromatography A, 1218  (2011) :5774– 5786. (SCI, IF = 4.356) （National Key Laboratory of Natural Drug Active Components and Pharmaceutical Effects of China Pharmaceutical University）

4、Microwave-assisted growth of In 2 O 3 nanoparticles on WO 3 nanoplates to improve H2S-sensing performance .Journal of Materials Chemistry A.2014, 2, 18867–18874 | 18867   (SCI,IF Influencing factors=6.626) （School of Materials Science and Engineering, Zhengzhou University）